Technology Process of C29H27NO6
There total 5 articles about C29H27NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium fluoride; tetrabutylammomium bromide; palladium diacetate;
In
water;
at 150 ℃;
for 0.25h;
Microwave irradiation;
DOI:10.1021/ja312148q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 15 h / 20 °C / Inert atmosphere
2.1: triethylamine; palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C
3.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C
3.2: 0.67 h / 0 °C
3.3: 2.6 h / 0 - 20 °C
4.1: potassium fluoride; tetrabutylammomium bromide; palladium diacetate / water / 0.25 h / 150 °C / Microwave irradiation
With
pyridine; hydrogenchloride; potassium fluoride; palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; palladium diacetate; triethylamine;
In
tetrahydrofuran; water; ethyl acetate;
3.2: |Sandmeyer Reaction / 3.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C
1.2: 0.67 h / 0 °C
1.3: 2.6 h / 0 - 20 °C
2.1: potassium fluoride; tetrabutylammomium bromide; palladium diacetate / water / 0.25 h / 150 °C / Microwave irradiation
With
hydrogenchloride; potassium fluoride; tetrabutylammomium bromide; palladium diacetate;
In
tetrahydrofuran; water;
1.2: |Sandmeyer Reaction / 1.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q
