2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

Base Information

Chemical Name:2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene
CAS No.:150333-54-3
Molecular Formula:C₃₃H₃₆N₄O₉S₃
Molecular Weight:728.868
Hs Code.:

Synonyms:2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

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Chemical Property of 2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

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Technology Process of 2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

There total 6 articles about 2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 16695-22-0
N,N-bis(tosyloxyethyl)-p-toluenesulfonamide

: 138572-08-4
4-Nitro-2-(p-toluenesulfonamido)-1-<2'-(p-toluenesulfonamido)ethoxy>benzene

: 150333-54-3
2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; for 10h;
DOI:10.1021/jo00069a034

Reference yield:

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 150333-54-3
2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / K₂CO₃ / dimethylformamide / 1.) 60 deg C, 5 min, 2.) 60 deg C, 24 h

2: 57 percent / Cs₂CO₃ / dimethylformamide / 10 h

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00069a034

Reference yield:

: 91956-17-1
N-(2-hydroxy-5-nitrophenyl)-4-methylbenzenesulfonamide

: 150333-54-3
2-Nitro-8,11,14-tris-(toluene-4-sulfonyl)-7,8,9,10,11,12,13,14-octahydro-6H-5-oxa-8,11,14-triaza-benzocyclododecene

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / K₂CO₃ / dimethylformamide / 1.) 60 deg C, 5 min, 2.) 60 deg C, 24 h

2: 57 percent / Cs₂CO₃ / dimethylformamide / 10 h

With potassium carbonate; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00069a034