1-(2-Methoxy-3-methylphenyl)-1-propanone

Base Information

Chemical Name:1-(2-Methoxy-3-methylphenyl)-1-propanone
CAS No.:68597-45-5
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:
DSSTox Substance ID:DTXSID101276677

Synonyms:68597-45-5;1-(2-methoxy-3-methylphenyl)-1-propanone;2-Methyl-6-propionylanisole;SCHEMBL9720578;DTXSID101276677

Suppliers and Price of 1-(2-Methoxy-3-methylphenyl)-1-propanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-Methoxy-3-methylphenyl)-1-propanone

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:178.099379685
Heavy Atom Count:13
Complexity:177

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(=O)C1=CC=CC(=C1OC)C

Technology Process of 1-(2-Methoxy-3-methylphenyl)-1-propanone

There total 9 articles about 1-(2-Methoxy-3-methylphenyl)-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 107076-03-9
1-(5-chloro-2-methoxy-3-methylphenyl)-1-propanone

: 68597-45-5
1-(2-methoxy-3-methylphenyl)-1-propanone

Guidance literature:: With potassium hydroxide; ammonium formate; palladium on activated charcoal; In ethanol; at 60 ℃; for 0.333333h;
DOI:10.1248/cpb.45.728

Reference yield:

: 1570-64-5
2-methyl-4-chlorophenol

: 68597-45-5
1-(2-methoxy-3-methylphenyl)-1-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) AlCl₃ / 1.) 80-90 deg C, 2 h, 2.) 80-90 deg C, 1 h

2: 74 percent / NaOH / ethanol / 2 h / Heating

3: 82 percent / 2.5 N aq. KOH, ammonium formate / 10percent Pd/C / ethanol / 0.33 h / 60 °C

With potassium hydroxide; sodium hydroxide; aluminium trichloride; ammonium formate; palladium on activated charcoal; In ethanol;
DOI:10.1248/cpb.45.728

Reference yield:

: 941-74-2
1-(5-chloro-2-hydroxy-3-methylphenyl)-1-propanone

: 68597-45-5
1-(2-methoxy-3-methylphenyl)-1-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaOH / ethanol / 2 h / Heating

2: 82 percent / 2.5 N aq. KOH, ammonium formate / 10percent Pd/C / ethanol / 0.33 h / 60 °C

With potassium hydroxide; sodium hydroxide; ammonium formate; palladium on activated charcoal; In ethanol;
DOI:10.1248/cpb.45.728