(p-Chlorobenzyl)vinyl sulfone

Base Information

Chemical Name:(p-Chlorobenzyl)vinyl sulfone
CAS No.:73927-12-5
Molecular Formula:C₉H₉ClO₂S
Molecular Weight:216.688
Hs Code.:
Mol file:73927-12-5.mol

Synonyms:p-Chlorobenzyl vinyl sulfone;Sulfone,p-chlorobenzyl vinyl;

Suppliers and Price of (p-Chlorobenzyl)vinyl sulfone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (p-Chlorobenzyl)vinyl sulfone

Chemical Property:

Vapor Pressure:6.14E-06mmHg at 25°C
Boiling Point:390°Cat760mmHg
Flash Point:189.7°C
PSA：42.52000
Density:1.298g/cm³
LogP:3.47910

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (p-Chlorobenzyl)vinyl sulfone

There total 3 articles about (p-Chlorobenzyl)vinyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₁₀BrClO₂S

: 73927-12-5
1-chloro-4-((vinylsulfonyl)methyl)benzene

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b02867

Reference yield:

: 6258-66-8
(4-chlorophenyl)methanethiol

: 73927-12-5
1-chloro-4-((vinylsulfonyl)methyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile / 18 h / 20 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

With caesium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;
DOI:10.1021/acs.orglett.9b02867

Reference yield:

: C₉H₁₀BrClS

: 73927-12-5
1-chloro-4-((vinylsulfonyl)methyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 18 h / 20 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/acs.orglett.9b02867