(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

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Chemical Name:(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene
CAS No.:1453119-90-8
Molecular Formula:C₇₈H₁₃₀N₄O₁₀S₃
Molecular Weight:1380.11
Hs Code.:

Synonyms:(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

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Chemical Property of (E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

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Technology Process of (E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

There total 4 articles about (E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1453119-89-5
(E,E,E)-1,14-dibromo-5,10-bis{[(3,4-didodecyloxy)phenyl]sulfonyl}-5,10-diazatetradeca-2,7,12-triene

: 63-74-1
sulfanilamide

: 1453119-90-8
(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

Guidance literature:: (E,E,E)-1,14-dibromo-5,10-bis{[(3,4-didodecyloxy)phenyl]sulfonyl}-5,10-diazatetradeca-2,7,12-triene; With potassium carbonate; In acetonitrile; at 70 ℃; for 0.25h;

sulfanilamide; In tetrahydrofuran; acetonitrile; at 70 ℃; Reflux;
DOI:10.1002/ejoc.201300222

Reference yield:

: N-(tert-butyloxycarbonyl)-3,4-bis(dodecyloxy)benzenesulfonamide

: 1453119-90-8
(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile

2.1: trifluoroacetic acid / dichloromethane / 6 h

3.1: potassium carbonate / acetonitrile; tetrahydrofuran / 0.25 h / 60 °C

3.2: Reflux

4.1: potassium carbonate / acetonitrile / 0.25 h / 70 °C

4.2: 70 °C / Reflux

With potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201300222

Reference yield:

: 3,4-bis(dodecyloxy)benzenesulfonamide

: 1453119-90-8
(E,E,E)-1-[(4-aminophenyl)sulfonyl]-6,11-bis{[(3,4-didodecyloxy)-phenyl]sulfonyl}-1,6,11-triazacyclopentadeca-3,8,13-triene

Guidance literature:: Multi-step reaction with 5 steps

1.1: dmap; triethylamine / dichloromethane

2.1: potassium carbonate / acetonitrile

3.1: trifluoroacetic acid / dichloromethane / 6 h

4.1: potassium carbonate / acetonitrile; tetrahydrofuran / 0.25 h / 60 °C

4.2: Reflux

5.1: potassium carbonate / acetonitrile / 0.25 h / 70 °C

5.2: 70 °C / Reflux

With dmap; potassium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201300222