4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

Base Information

Chemical Name:4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside
CAS No.:1621691-98-2
Molecular Formula:C₁₈H₂₅N₃O₁₀
Molecular Weight:443.411
Hs Code.:

Synonyms:4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

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Chemical Property of 4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

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Technology Process of 4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

There total 15 articles about 4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1621691-97-1
4-(2-azidoethoxy)phenyl 3,5-di-O-benzoyl-2-O-[β-D-arabinofuranosyl]-α-D-arabinofuranoside

: 1621691-98-2
4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: 4-(2-azidoethoxy)phenyl 3,5-di-O-benzoyl-2-O-[β-D-arabinofuranosyl]-α-D-arabinofuranoside; With sodium methylate; In methanol; at 20 ℃; for 48h;

In water; for 0.166667h;
DOI:10.1016/j.carres.2014.05.017

Reference yield:

: 1621691-96-0
C₃₂H₃₃N₃O₁₂

: 1621691-98-2
4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: C₃₂H₃₃N₃O₁₂; With sodium methylate; In methanol; at 20 ℃; for 48h;

In methanol;
DOI:10.1016/j.carres.2014.05.017

Reference yield:

: 1621691-95-9
4-(2-chloroethoxy)phenyl 3,5-di-O-benzoyl-2-O-[β-D-arabinofuranosyl]-α-D-arabinofuranoside

: 1621691-98-2
4-(2-azidoethoxy)phenyl 2-O-(β-D-arabinofuranosyl)-α-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide; 18-crown-6 ether / N,N-dimethyl-formamide / 48 h / 80 °C

2.1: sodium methylate / methanol / 48 h / 20 °C

2.2: Dowex 50Wx₄ (PyH⁺) / 0.17 h

With sodium azide; 18-crown-6 ether; sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2014.05.017