<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

Base Information

Chemical Name:<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione
CAS No.:132523-68-3
Molecular Formula:C₂₄H₂₆N₂O₅
Molecular Weight:422.481
Hs Code.:

<3S-(3α,4β,5α)>-1-<tetrahydro-4,5-bis<(phenylmethoxy)methyl>-3-furanyl>-2,4(1H,3H)-pyrimidinedione

Synonyms:<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

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Chemical Property of <3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

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Technology Process of <3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

There total 8 articles about <3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 161452-70-6
(2R,3R)-1,4-anhydro-5-O-benzyl-3-C-benzyloxymethyl-2,3-dideoxy-2--D-arabitol

: 132523-68-3
<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

Guidance literature:: With sulfuric acid; In 1,4-dioxane; at 100 ℃; for 2h;
DOI:10.1016/S0040-4020(01)81749-X

Reference yield: 28.0%

: 66-22-8,144104-68-7,18324-22-6,27072-01-1,2920-92-5,51953-19-6
uracil

: 132523-63-8
1,3-dideoxy-3-<(phenylmethoxy)methyl>-5-O-(phenylmethyl)-D-ribofuranose 2-(4-methylbenzenesulfonate)

: 1,4-anhydro-5-O-benzyl-3-C-benzyloxymethyl-2,3-didehydro-2,3-dideoxy-D-ribo-pentitol

: 132523-68-3
<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In dimethyl sulfoxide; at 90 ℃; for 7.5h;
DOI:10.1021/jm00061a013

Reference yield:

: 132617-86-8
1,3-dideoxy-3-<(phenylmethoxy)methyl>-5-O-(phenylmethyl)-D-ribofuranose

: 132523-68-3
<3S-(3α,4β,5α)>-1--3-furanyl>-2,4(1H,3H)-pyrimidinedione

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / DMAP, Et₃N / CH₂Cl₂ / Ambient temperature

2: 93 percent / LiN₃ / dimethylformamide / 100 °C

3: 96 percent / H₂ / Lindlar catalyst / methanol; ethyl acetate / Ambient temperature

4: 99 percent / benzene; dimethylformamide / 1.) -18 deg C; 2.) RT

5: 90 percent / 2N H₂SO₄ / dioxane / 2 h / 100 °C

With dmap; lithium azide; sulfuric acid; hydrogen; triethylamine; Lindlar's catalyst; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(01)81749-X