⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester

Base Information

• Chemical Name: ⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester
• CAS No.: 1258980-66-3
• Molecular Formula: C₃₁H₄₉IN₄O₈
• Molecular Weight: 728.752

Synonyms:⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester

Chemical Property of ⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester

Chemical Property:

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Technology Process of ⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester

There total 1 articles about ⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-di-tert-butyl 2-(3-((S)-1-tert-butoxy-1-oxo-6-(3-(4-(trimethylstannyl)phenyl)ureido)hexan-2-yl)ureido)pentanedioate (949575-23-9) → (123)I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester (1258980-66-3)

Guidance literature:

With [¹²³I] sodium iodide; sulfuric acid; dihydrogen peroxide; acetic acid; In water; acetonitrile; at 20 ℃; for 0.183333h; Inert atmosphere;

DOI:10.1021/jm800994j

Reference yield:

(123)I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)-pentyl)ureido)pentanedioic acid tri-tert-butyl ester (1258980-66-3) → (123)I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)pentyl)ureido)pentanedioic acid (949575-25-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.75h; Inert atmosphere;

DOI:10.1021/jm800994j

upstream raw materials:

(S)-di-tert-butyl 2-(3-((S)-1-tert-butoxy-1-oxo-6-(3-(4-(trimethylstannyl)phenyl)ureido)hexan-2-yl)ureido)pentanedioate

Downstream raw materials:

⁽¹²³⁾I-(S)-2-(3-((S)-1-carboxy-5-(3-(4-iodophenyl)ureido)pentyl)ureido)pentanedioic acid

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