(3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine

Base Information

• Chemical Name: (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine
• CAS No.: 866467-38-1
• Molecular Formula: C₁₅H₂₂N₂
• Molecular Weight: 230.353

Synonyms:(3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine

Chemical Property of (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine

Chemical Property:

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Technology Process of (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine

There total 2 articles about (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(3aR,6S,6aS)-6-azido-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrole (1131006-66-0) → (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine (866467-38-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 4h; under 760.051 Torr;

DOI:10.1021/jm801450c

Reference yield:

C15H20IN → (3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine (866467-38-1) + (3aS,6R,6aR)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine (1131006-64-8)

Guidance literature:

With ammonium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 17h;

DOI:10.1021/jm801450c

Reference yield: 65.0%

(3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-ylamine (866467-38-1) + 2-(Trimethylsilyl)ethyl 4-nitrophenyl carbonate (80149-80-0) → [(3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-yl]carbamic acid 2-trimethylsilanylethyl ester (1131006-67-1)

Guidance literature:

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 14h;

DOI:10.1021/jm801450c

upstream raw materials:

(3aR,6S,6aS)-6-azido-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrole

Downstream raw materials:

[(3aR,6S,6aS)-1-((R)-1-phenylethyl)octahydrocyclopenta[b]pyrrol-6-yl]carbamic acid 2-trimethylsilanylethyl ester

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