C₂₆H₂₃N₃O₅S

Base Information

Chemical Name:C₂₆H₂₃N₃O₅S
CAS No.:1181080-54-5
Molecular Formula:C₂₆H₂₃N₃O₅S
Molecular Weight:489.552
Hs Code.:

C<sub>26</sub>H<sub>23</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₆H₂₃N₃O₅S

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Chemical Property of C₂₆H₂₃N₃O₅S

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Technology Process of C₂₆H₂₃N₃O₅S

There total 18 articles about C₂₆H₂₃N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1181080-53-4
C₃₂H₃₇N₃O₅SSi

: 1181080-54-5
C₂₆H₂₃N₃O₅S

Guidance literature:: C₃₂H₃₇N₃O₅SSi; With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 7h; Inert atmosphere;

With water; sodium hydrogencarbonate; In dichloromethane; Inert atmosphere;
DOI:10.1021/ol901471r

Reference yield:

: 55149-84-3
2-nitroveratraldehyde

: 1181080-54-5
C₂₆H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium hydroxide / ethanol; N,N-dimethyl-formamide / 1.25 h / -2 °C

2.1: palladium on carbon; formic acid; ammonium formate / methanol / 1 h

3.1: 2 h / 0 °C

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / Reflux

5.1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 9 h

6.1: potassium tert-butylate / tetrahydrofuran / 6 h / 0 °C

7.1: 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; bis-[(trifluoroacetoxy)iodo]benzene / water / 1 h / 0 °C

8.1: hydrogenchloride / methanol / 0.5 h / 20 °C / Inert atmosphere

8.2: 16 h / 20 °C / Inert atmosphere

9.1: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 0.5 h / 20 °C / Inert atmosphere

10.1: boron trifluoride diethyl etherate / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; formic acid; 1,1,1,3',3',3'-hexafluoro-propanol; trimethylsilyl trifluoromethanesulfonate; diphenyl phosphoryl azide; palladium on carbon; boron trifluoride diethyl etherate; potassium tert-butylate; ammonium formate; triphenylphosphine; bis-[(trifluoroacetoxy)iodo]benzene; potassium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; 2,2,2-trifluoroethanol; water; N,N-dimethyl-formamide; toluene; 5.1: Mitsunobu reaction;
DOI:10.1039/c1ob05058c

Reference yield:

: 1181080-76-1
C₂₈H₂₇NO₂

: 1181080-54-5
C₂₆H₂₃N₃O₅S

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2.5 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

3.1: hydrogenchloride / methanol / 0.5 h / 20 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

4.1: bis-[(trifluoroacetoxy)iodo]benzene / 2,2,2-trifluoroethanol / 0.5 h / 20 °C / Inert atmosphere

5.1: boron trifluoride diethyl etherate / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; methanol; dichloromethane; 2,2,2-trifluoroethanol;
DOI:10.1039/c1ob05058c