(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

Base Information

Chemical Name:(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester
CAS No.:100009-07-2
Molecular Formula:C₂₂H₁₉N₃O₃
Molecular Weight:373.411
Hs Code.:

Synonyms:(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

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Chemical Property of (S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

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Technology Process of (S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

There total 3 articles about (S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 74214-63-4
β-carboline-3-carboxylic acid

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 100009-07-2
(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

Guidance literature:: With 1,1'-carbonyldiimidazole; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1002/jps.2600740620

Reference yield:

: 69954-48-9
methyl 9H-β-carboline-3-carboxylate

: 100009-07-2
(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / Pb(OAc)4 / acetic acid / 1 h

2: 96 percent / NaOH / ethanol; H₂O / 0.5 h / Heating

3: 75 percent / 1,1'-carbonyldiimidazole / dimethylformamide / Ambient temperature

With lead(IV) acetate; sodium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600740620

Reference yield:

: 100009-00-5
methyl-β-carboline-3-carboxylate hydrogen oxalate

: 100009-07-2
(S)-2-[(9H-β-Carboline-3-carbonyl)-amino]-3-phenyl-propionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NaOH / ethanol; H₂O / 0.5 h / Heating

2: 75 percent / 1,1'-carbonyldiimidazole / dimethylformamide / Ambient temperature

With sodium hydroxide; 1,1'-carbonyldiimidazole; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1002/jps.2600740620