1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

Base Information

Chemical Name:1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate
CAS No.:1007579-22-7
Molecular Formula:C₂₉H₄₀N₂O₄
Molecular Weight:480.648
Hs Code.:

Synonyms:1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

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Chemical Property of 1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

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Technology Process of 1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

There total 8 articles about 1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1007579-11-4
1,1-dimethylethyl {2-[(4-bromophenyl)oxy]ethyl}(4,4-dimethylcyclohexyl)carbamate

: 101251-09-6
(4-acetylaminophenyl)boronic acid

: 1007579-22-7
1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 1.17h; Inert atmosphere;

Reference yield:

PdCl₂(dppf).CH₂Cl₂: PdCl₂(dppf).CH₂Cl₂

: 1007579-11-4
1,1-dimethylethyl {2-[(4-bromophenyl)oxy]ethyl}(4,4-dimethylcyclohexyl)carbamate

: 101251-09-6
(4-acetylaminophenyl)boronic acid

: 1007579-22-7
1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

Guidance literature:: With sodium carbonate; In 1,2-dimethoxyethane;

Reference yield:

: 1073-13-8
4,4-dimethylcyclohexenone

: 1007579-22-7
1,1-dimethylethyl (2-{[4′-(acetylamino)-4-biphenylyl]oxy}ethyl)(4,4-dimethylcyclohexyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 3 h / 20 °C / 775.74 Torr

2: acetic acid; sodium cyanoborohydride / methanol / 20 °C

3: triethylamine / dichloromethane / 13 h

4: sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / N,N-dimethyl-formamide / 1.17 h / 20 - 80 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium 10% on activated carbon; hydrogen; sodium cyanoborohydride; sodium carbonate; acetic acid; triethylamine; In methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 4: |Suzuki Coupling;