4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride

Base Information

• Chemical Name: 4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride
• CAS No.: 1169394-30-2
• Molecular Formula: C₂₂H₂₀ClN₅O*ClH
• Molecular Weight: 444.337

Synonyms:4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride

Chemical Property of 4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride

Chemical Property:

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Technology Process of 4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride

There total 1 articles about 4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-⁽¹⁴⁾C-nitrile hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

zinc [14C2]cyanide + 4-(1-[(4-bromophenyl)methyl]imidazol-5-ylmethyl)-1-(3-chlorophenyl)piperazin-2-one (312936-83-7) → 4-[(5-[4-(3-chlorophenyl)-3-oxopiperazinyl]methylimidazol-1-yl)methyl]benzenecarbo-(14)C-nitrile hydrochloride (1169394-30-2)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 70 ℃; for 20h;

DOI:10.1002/jlcr.1545

upstream raw materials:

4-(1-[(4-bromophenyl)methyl]imidazol-5-ylmethyl)-1-(3-chlorophenyl)piperazin-2-one

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