C₂₂H₂₂N₆O₂

Base Information

Chemical Name:C₂₂H₂₂N₆O₂
CAS No.:1431701-49-3
Molecular Formula:C₂₂H₂₂N₆O₂
Molecular Weight:402.456
Hs Code.:

C<sub>22</sub>H<sub>22</sub>N<sub>6</sub>O<sub>2</sub>

Synonyms:C₂₂H₂₂N₆O₂

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Chemical Property of C₂₂H₂₂N₆O₂

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Technology Process of C₂₂H₂₂N₆O₂

There total 8 articles about C₂₂H₂₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: C₂₄H₂₆N₆O₂

: 1431701-49-3
C₂₂H₂₂N₆O₂

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1431701-49-3
C₂₂H₂₂N₆O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

5.1: potassium carbonate; methanol / 2 h / 20 °C

6.1: sodium azide; acetic acid / 0.17 h / 5 °C

7.1: sodium hydroxide / tetrahydrofuran / 18 h / 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; palladium diacetate; sodium hydride; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; acetic acid; triethylamine; sodium hydroxide; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1431701-49-3
C₂₂H₂₂N₆O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

5.1: potassium carbonate; methanol / 2 h / 20 °C

6.1: sodium azide; acetic acid / 0.17 h / 5 °C

7.1: sodium hydroxide / tetrahydrofuran / 18 h / 20 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; palladium diacetate; sodium hydride; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; acetic acid; triethylamine; sodium hydroxide; sodium t-butanolate; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide; N,N-dimethyl-formamide;