(2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

Base Information

Chemical Name:(2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate
CAS No.:1087342-94-6
Molecular Formula:C₃₉H₅₄O₇
Molecular Weight:634.854
Hs Code.:

Synonyms:(2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

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Technology Process of (2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

There total 1 articles about (2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1087342-86-6
C₈H₁₄O₃S

: 1087342-93-5
C₃₂H₄₂O₇

: 1087343-11-0
2-(3-ethynyl-2-hydroxy-5-methylhexyl)-8-(-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

: 1087342-94-6
(2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

Guidance literature:: With diethylzinc; palladium diacetate; triphenylphosphine; In tetrahydrofuran; hexane; at -78 - -20 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ja807127s

Reference yield: 100.0%

: 1087342-94-6
(2S,3S,4R,6R,8S)-2-((2R,3S)-3-ethynyl-2-hydroxy-5-methylhexyl)-8-((R)-2-(4-methoxybenzyloxy)butyl)-3,9-dimethyl-1,7-dioxaspiro-[5.5]undecan-4-yl benzoate

: 69739-34-0
t-butyldimethylsiyl triflate

: 1087343-12-1
C₄₅H₆₈O₇Si

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja807127s DOI:10.1021/ja906056v