2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile

Base Information

• Chemical Name: 2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile
• CAS No.: 1092584-80-9
• Molecular Formula: C₂₂H₂₁N₃O₂
• Molecular Weight: 359.428

Synonyms:2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile

Chemical Property of 2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile

Chemical Property:

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Technology Process of 2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile

There total 1 articles about 2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

3-benzyl-6-(2-bromobenzylidene)-1,3,4-trimethylpiperazine-2,5-dione (1092584-79-6) + copper(l) cyanide → 2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile (1092584-80-9)

Guidance literature:

In 1-Methylpyrrolidine; at 155 ℃; for 16h;

Reference yield:

2-(5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylidenemethyl)-benzonitrile (1092584-80-9) → (S,S)-2-[5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylmethyl]benzonitrile (1092585-25-5) + (R,S)-2-[5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylmethyl]benzonitrile

Guidance literature:

With hydrogen; 10% palladium on carbon; In methanol; for 7h;

upstream raw materials:

3-benzyl-6-(2-bromobenzylidene)-1,3,4-trimethylpiperazine-2,5-dione

Downstream raw materials:

(S,S)-2-[5-benzyl-1,4,5-trimethyl-3,6-dioxopiperazin-2-ylmethyl]benzonitrile

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