N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Base Information

Chemical Name:N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide
CAS No.:23742-45-2
Molecular Formula:C₁₁H₉BrF₃NO
Molecular Weight:308.098
Hs Code.:

Synonyms:N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

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Chemical Property of N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

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Technology Process of N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

There total 1 articles about N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 454-79-5
2-Bromo-5-trifluoromethylaniline

: 4023-34-1
cyclopropanecarboxylic acid chloride

: 23742-45-2
N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: 2-Bromo-5-trifluoromethylaniline; cyclopropanecarboxylic acid chloride; With triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h; Inert atmosphere;

With dmap; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol400380y

Reference yield:

: 23742-45-2
N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

: 1426327-92-5
N-(2-bromo-5-(trifluoromethyl)phenyl)-N-(cyclopropylmethyl)-1,1,1-trifluoromethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: diborane / tetrahydrofuran / 8 h / Inert atmosphere; Reflux

2.1: sodium hydride / 1,2-dichloro-ethane / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With sodium hydride; diborane; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/ol400380y