C₃₀H₄₈O₈Si

Base Information

Chemical Name:C₃₀H₄₈O₈Si
CAS No.:1449375-05-6
Molecular Formula:C₃₀H₄₈O₈Si
Molecular Weight:564.792
Hs Code.:

C<sub>30</sub>H<sub>48</sub>O<sub>8</sub>Si

Synonyms:C₃₀H₄₈O₈Si

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Chemical Property of C₃₀H₄₈O₈Si

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Technology Process of C₃₀H₄₈O₈Si

There total 19 articles about C₃₀H₄₈O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1449375-04-5
C₂₄H₃₄O₈

: 151073-99-3
(2-trimethylsilylprop-2-en-1-yl)tributylstannane

: 1449375-05-6
C₃₀H₄₈O₈Si

Guidance literature:: (2-trimethylsilylprop-2-en-1-yl)tributylstannane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

C₂₄H₃₄O₈; In tetrahydrofuran; hexane; at -78 ℃; for 1h;
DOI:10.1016/j.tet.2013.05.067

Reference yield:

: C₂₆H₃₄O₅Si

: 1449375-05-6
C₃₀H₄₈O₈Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: diisobutylaluminium hydride / toluene; hexane / -78 - 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 3 h / 0 - 20 °C

4.1: AD-mix-β; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium osmate(VI) dihydrate; methanesulfonamide / tert-butyl alcohol / pH 7

5.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

7.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -60 °C

7.2: -60 - 20 °C

8.1: potassium tert-butylate / tetrahydrofuran / -10 - 20 °C

8.2: -10 - 20 °C

9.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); potassium carbonate; potassium osmate(VI) dihydrate; methanesulfonamide / tert-butyl alcohol / pH 7

10.1: pyridinium p-toluenesulfonate; Trimethyl orthoacetate / dichloromethane / 2 h / 20 °C

10.2: 5 h / 20 °C

10.3: 20 °C

11.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

11.2: 1 h / -78 °C

With Trimethyl orthoacetate; potassium osmate(VI) dihydrate; n-butyllithium; oxalyl dichloride; methanesulfonamide; AD-mix-β; potassium tert-butylate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; hydroquinidein 1,4-phthalazinediyl diether; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In tetrahydrofuran; hexane; dichloromethane; acetone; toluene; tert-butyl alcohol; 4.1: |Sharpless Dihydroxylation / 7.1: |Swern Oxidation / 7.2: |Swern Oxidation / 9.1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tet.2013.05.067

Reference yield:

: 1449374-89-3
(2R,3S,4R,5S,6R)-2-(2-methylprop-1-en-1-yl)-6-((tert-butyldiphenylsilyloxy)methyl)tetrahydro-2H-pyran-3,4,5-triol

: 1449375-05-6
C₃₀H₄₈O₈Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C

2.1: 1H-imidazole; sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C

2.2: 0.5 h / 20 °C

2.3: 0.17 h

3.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / benzene / 2.5 h / 60 °C / Reflux

4.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tert-butyl alcohol / 20 °C / pH 7

4.2: 3407 / 4 h / 20 °C / pH 7

5.1: dichloromethane / 1 h / 20 °C

6.1: diisobutylaluminium hydride / toluene; hexane / -78 - 0 °C

7.1: potassium tert-butylate / tetrahydrofuran / 3 h / 0 - 20 °C

8.1: AD-mix-β; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium osmate(VI) dihydrate; methanesulfonamide / tert-butyl alcohol / pH 7

9.1: toluene-4-sulfonic acid / acetone / 4 h / 0 - 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 0 - 20 °C

11.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -60 °C

11.2: -60 - 20 °C

12.1: potassium tert-butylate / tetrahydrofuran / -10 - 20 °C

12.2: -10 - 20 °C

13.1: hydroquinidein 1,4-phthalazinediyl diether; potassium hexacyanoferrate(III); potassium carbonate; potassium osmate(VI) dihydrate; methanesulfonamide / tert-butyl alcohol / pH 7

14.1: pyridinium p-toluenesulfonate; Trimethyl orthoacetate / dichloromethane / 2 h / 20 °C

14.2: 5 h / 20 °C

14.3: 20 °C

15.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

15.2: 1 h / -78 °C

With 1H-imidazole; Trimethyl orthoacetate; potassium osmate(VI) dihydrate; osmium(VIII) oxide; n-butyllithium; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); methanesulfonamide; AD-mix-β; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; hydroquinidein 1,4-phthalazinediyl diether; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In tetrahydrofuran; hexane; dichloromethane; acetone; toluene; mineral oil; tert-butyl alcohol; benzene; 3.1: |Barton-McCombie Deoxygenation / 8.1: |Sharpless Dihydroxylation / 11.1: |Swern Oxidation / 11.2: |Swern Oxidation / 13.1: |Sharpless Dihydroxylation;
DOI:10.1016/j.tet.2013.05.067