Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

Base Information

Chemical Name:Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid
CAS No.:146597-51-5
Molecular Formula:C₄₅H₆₇NO₂₀
Molecular Weight:942.022
Hs Code.:

Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

Synonyms:Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

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Chemical Property of Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

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Technology Process of Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

There total 11 articles about Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 146597-69-5
Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-4,6-O-isopropyliden-β-D-mannopyranosid

: 146597-51-5
Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

Guidance literature:: With acetic acid; for 3h; Ambient temperature;

Reference yield:

: 139493-89-3
Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(3,4,6-tri-O-acetyl-α-D-mannopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

: 146597-51-5
Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 9 steps

1: molecular sieves 3 Angstroem, BF₃*OEt₂ / CH₂Cl₂ / 2 h / -20 deg C to r.t.

2: pyridine / 12 h / Ambient temperature

3: hydrogen / 10 percent Pd/C / methanol; ethyl acetate / 8 h / 760 Torr

4: pyridine / 7 h / Ambient temperature

5: 91 percent / Bu₃SnH, AIBN / dioxane; toluene / 1 h / 90 °C

6: 80 percent acetic acid / 3 h / Ambient temperature

7: pyridine / 7 h

9: 100 percent / 80 percent aq. acetic acid / 3 h / Ambient temperature

With pyridine; 2,2'-azobis(isobutyronitrile); 3 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; tri-n-butyl-tin hydride; acetic acid; palladium on activated charcoal; In 1,4-dioxane; methanol; dichloromethane; ethyl acetate; toluene;

Reference yield:

: C₅₉H₈₅NO₂₉

: 146597-51-5
Octyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-(1->2)-O-(4,6-di-O-acetyl-3-desoxy-α-D-arabino-hexopyranosyl)-(1->3)-2-O-benzyl-β-D-mannopyranosid

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / 12 h / Ambient temperature

2: hydrogen / 10 percent Pd/C / methanol; ethyl acetate / 8 h / 760 Torr

3: pyridine / 7 h / Ambient temperature

4: 91 percent / Bu₃SnH, AIBN / dioxane; toluene / 1 h / 90 °C

5: 80 percent acetic acid / 3 h / Ambient temperature

6: pyridine / 7 h

8: 100 percent / 80 percent aq. acetic acid / 3 h / Ambient temperature

With pyridine; 2,2'-azobis(isobutyronitrile); hydrogen; tri-n-butyl-tin hydride; acetic acid; palladium on activated charcoal; In 1,4-dioxane; methanol; ethyl acetate; toluene;