((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄

Base Information

• Chemical Name: ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄
• CAS No.: 96454-65-8
• Molecular Formula: BF₄*C₃₉H₄₀O₂P₃W
• Molecular Weight: 904.321

Synonyms:((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄

Chemical Property of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄

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Technology Process of ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄

There total 1 articles about ((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2((CH₃)3P)BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

[((C6H5)2PCH2)2W(CCH2C6H5)(CO)2](1+)*BF4(1-)=((C6H5)2PCH2CH2P(C6H5)2)W(CCH2C6H5)(CO)2BF4 (96454-61-4) + trimethylphosphane (594-09-2) → ((C6H5)2PCH2CH2P(C6H5)2)W(CCH2C6H5)(CO)2((CH3)3P)(1+)*BF4(1-)=((C6H5)2PCH2CH2P(C6H5)2)W(CCH2C6H5)(CO)2((CH3)3P)BF4 (96454-65-8)

Guidance literature:

In dichloromethane; a soln. of the complex cooling to -78°C, 1 equiv of PMe3 adding under N2, stirring for 15 min at -78°C, warming to room temp., stirring for 1 h, concg., Et2O-hexane adding, cooling to -20°C, crystals sepg., washing with hexane; identified by IR and NMR spectra;

DOI:10.1021/ja00301a017

upstream raw materials:

[((C₆H₅)2PCH₂)2W(CCH₂C₆H₅)(CO)2]⁽¹⁺⁾*BF₄^(1-)=((C₆H₅)2PCH₂CH₂P(C₆H₅)2)W(CCH₂C₆H₅)(CO)2BF₄

trimethylphosphane

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