Technology Process of C18H23NO6
There total 7 articles about C18H23NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-Allyl-4-phenyl-1,3-oxazolidin-2-one;
With
dimethylsulfide; ozone;
In
dichloromethane;
at -78 - 20 ℃;
2-methyl-but-2-ene;
With
sodium chlorite; sodium dihydrogenphosphate;
In
water; tert-butyl alcohol;
for 4h;
methanol; bromoacetic acid tert-butyl ester;
With
hydrogenchloride; sodium hydride;
more than 3 stages;
Product distribution / selectivity;
- Guidance literature:
-
C12H13NO4; bromoacetic acid tert-butyl ester;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
With
water; ammonium chloride;
In
tetrahydrofuran;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 4 h / 0 - 20 °C
2: sodium periodate / ruthenium trichloride / dichloromethane; water; acetonitrile / 5 h / 20 °C
3: hydrogenchloride / 20 - 35 °C / Heating / reflux
4: sodium hydride / tetrahydrofuran / 0 - 20 °C
With
sodium periodate; sodium hydride; triethylamine;
hydrogenchloride; ruthenium trichloride;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;