C₄₇H₇₀O₁₃

Base Information

Chemical Name:C₄₇H₇₀O₁₃
CAS No.:1351619-45-8
Molecular Formula:C₄₇H₇₀O₁₃
Molecular Weight:843.065
Hs Code.:

C<sub>47</sub>H<sub>70</sub>O<sub>13</sub>

Synonyms:C₄₇H₇₀O₁₃

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Chemical Property of C₄₇H₇₀O₁₃

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Technology Process of C₄₇H₇₀O₁₃

There total 10 articles about C₄₇H₇₀O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 42599-18-8
(E)-1-hexenyldihydroxyborane

: 1351619-35-6
C₄₁H₅₉BrO₁₃

: 1351619-45-8
C₄₇H₇₀O₁₃

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; cesium fluoride; In 1,4-dioxane; at 60 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-56-1
C₂₂H₃₃BrO₇

: 1351619-45-8
C₄₇H₇₀O₁₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium triethylborohydride / tetrahydrofuran / 0 - 20 °C

2.1: 2,6-dimethylpyridine / dichloromethane / 22 h / 0 - 20 °C / Inert atmosphere

2.2: 2 h

3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

3.2: 1.5 h / 20 °C / Inert atmosphere

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

5.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; cesium fluoride / 1,4-dioxane / 2 h / 60 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 2,6-dimethylpyridine; 2,4,6-trichlorobenzoyl chloride; palladium diacetate; lithium triethylborohydride; pyridine hydrogenfluoride; triethylamine; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene; 5.1: Suzuki coupling;
DOI:10.1016/j.tet.2011.09.058

Reference yield:

: 1351619-36-7
C₃₄H₆₅BrO₆Si₃

: 1351619-45-8
C₄₇H₇₀O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 6 h / 20 °C / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: pyridine hydrogenfluoride / tetrahydrofuran / 5 h / 0 - 20 °C / Inert atmosphere

3.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; cesium fluoride / 1,4-dioxane / 2 h / 60 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 2,4,6-trichlorobenzoyl chloride; palladium diacetate; pyridine hydrogenfluoride; triethylamine; cesium fluoride; In tetrahydrofuran; 1,4-dioxane; toluene; 3.1: Suzuki coupling;
DOI:10.1016/j.tet.2011.09.058