1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene

Base Information

• Chemical Name: 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene
• CAS No.: 171253-95-5
• Molecular Formula: C₅₇H₆₀N₆O₉
• Molecular Weight: 973.138

Synonyms:1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene

Chemical Property of 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene

Chemical Property:

Purity/Quality:

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Technology Process of 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene

There total 2 articles about 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) + 1-(γ-aminopropyl)-3-benzyloxy-2-methyl-4-pyridinone (171253-88-6) → 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene (171253-95-5)

Guidance literature:

With triethylamine; In N,N-dimethyl acetamide; at 95 - 110 ℃; for 20h;

DOI:10.1080/00397919508015476

Reference yield:

Maltol (118-71-8) → 1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene (171253-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent

2: ethanol; H₂O / 168 h / Ambient temperature

3: Et₃N / N,N-dimethyl-acetamide / 20 h / 95 - 110 °C

With triethylamine; In ethanol; N,N-dimethyl acetamide; water;

DOI:10.1080/00397919508015476

Reference yield: 90.0%

1,3,5-tris<<γ-(3-benzyloxy-2-methyl-4-pyridinon-1-yl)propyl>carbamido>benzene (171253-95-5) → 1,3,5-tris<<γ-(3-hydroxy-2-methyl-4-pyridin-1-yl)propyl>carbamido>benzene

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 24h;

DOI:10.1080/00397919508015476

upstream raw materials:

1,3,5-benzene tris(carbonyl chloride)

1-(γ-aminopropyl)-3-benzyloxy-2-methyl-4-pyridinone

Maltol

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