N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

Base Information

Chemical Name:N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine
CAS No.:1384980-86-2
Molecular Formula:C₁₈H₁₉ClN₂O₅S
Molecular Weight:410.878
Hs Code.:

Synonyms:N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

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Technology Process of N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

There total 8 articles about N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1384980-58-8
N-[5-(2,5-dimethylphenoxy)-2,2-dimethylpentanoyl]-S-methyl-S-2-pyridylsulfoximine

: 64-19-7,77671-22-8
acetic acid

: 1384980-86-2
N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; at 60 ℃; for 24h;
DOI:10.1021/ol301579q

Reference yield:

: 1384980-51-1
N-[2,2-dimethyl-3-phenylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

: 1384980-86-2
N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

Guidance literature:: Multi-step reaction with 4 steps

1: [bis(acetoxy)iodo]benzene; palladium diacetate / acetic anhydride / 28 h / 70 °C

2: hydrogenchloride; water / 6 h / 50 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

4: [bis(acetoxy)iodo]benzene; palladium diacetate / 24 h / 60 °C

With hydrogenchloride; dmap; [bis(acetoxy)iodo]benzene; water; palladium diacetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetic anhydride;
DOI:10.1021/ol301579q

Reference yield:

: 18438-38-5,79639-75-1
2-methylsulfanyl-pyridine

: 1384980-86-2
N-[3-acetoxy-2-(4-chlorophenoxy)-2-methylpropanoyl]-S-methyl-S-2-pyridylsulfoximine

Guidance literature:: Multi-step reaction with 5 steps

1: dihydrogen peroxide / 20 °C

2: iron(III)-acetylacetonate; [bis(acetoxy)iodo]benzene / acetonitrile / 20 °C

3: caesium carbonate; thiophenol / acetonitrile / 20 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

5: [bis(acetoxy)iodo]benzene; palladium diacetate / 24 h / 60 °C

With dmap; iron(III)-acetylacetonate; [bis(acetoxy)iodo]benzene; dihydrogen peroxide; palladium diacetate; caesium carbonate; thiophenol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; acetonitrile;
DOI:10.1021/ol301579q