Technology Process of C29H27F3O6
There total 5 articles about C29H27F3O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; 1,10-Phenanthroline;
In
dimethyl sulfoxide;
at 70 ℃;
for 16h;
DOI:10.1021/ja312148q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C
1.2: 0.67 h / 0 °C
1.3: 2.6 h / 0 - 20 °C
2.1: copper(l) iodide; 1,10-Phenanthroline / dimethyl sulfoxide / 16 h / 70 °C
With
hydrogenchloride; copper(l) iodide; 1,10-Phenanthroline;
In
tetrahydrofuran; water; dimethyl sulfoxide;
1.2: |Sandmeyer Reaction / 1.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine / 15 h / 20 °C / Inert atmosphere
2.1: triethylamine; palladium 10% on activated carbon; hydrogen / ethyl acetate / 1 h / 20 °C
3.1: hydrogenchloride / tetrahydrofuran; water / 0.25 h / 0 °C
3.2: 0.67 h / 0 °C
3.3: 2.6 h / 0 - 20 °C
4.1: copper(l) iodide; 1,10-Phenanthroline / dimethyl sulfoxide / 16 h / 70 °C
With
pyridine; hydrogenchloride; copper(l) iodide; 1,10-Phenanthroline; palladium 10% on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; water; dimethyl sulfoxide; ethyl acetate;
3.2: |Sandmeyer Reaction / 3.3: |Sandmeyer Reaction;
DOI:10.1021/ja312148q