1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Base Information

Chemical Name:1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane
CAS No.:1346227-49-3
Molecular Formula:C₄₇H₄₅NO₈
Molecular Weight:751.876
Hs Code.:

Synonyms:1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

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Chemical Property of 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

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Technology Process of 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

There total 5 articles about 1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1346227-48-2
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-vinylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

: 1346227-49-3
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In chloroform; at 20 ℃; for 4h;

Reference yield:

: 4143-63-9
4'-hydroxyflavone

: 1346227-49-3
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / Reflux

2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

2.2: pH 10

3.1: potassium carbonate / acetonitrile / 3 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / chloroform / 4 h / 20 °C

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1346226-72-9
1,13-bis[4-(4H-chromen-4-on-2-yl)phenyl]-7-(tert-butyloxycarbonyl)-1,4,10,13-tetraoxa-7-azatridecane

: 1346227-49-3
1,13-bis[4'-(4H-chromen-4-on-2-yl)phenyl]-7-(4-ethylbenzyl)-1,4,10,13-tetraoxa-7-azatridecane

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

1.2: pH 10

2.1: potassium carbonate / acetonitrile / 3 h / Reflux

3.1: hydrogen / palladium 10% on activated carbon / chloroform / 4 h / 20 °C

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium 10% on activated carbon; In dichloromethane; chloroform; acetonitrile;