chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

Base Information

Chemical Name:chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane
CAS No.:1417537-03-1
Molecular Formula:C₂₇H₃₇ClOSi
Molecular Weight:441.129
Hs Code.:

Synonyms:chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

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Chemical Property of chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

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Technology Process of chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

There total 9 articles about chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1379658-32-8
2-methyl-4-methoxy-7-(3,5-di-tert-butylphenyl)-1H-indene

: 75-78-5,30107-43-8
dimethylsilicon dichloride

: 1417537-03-1
chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; toluene; at -20 - 60 ℃; for 16h;

Reference yield:

: 4-bromo-1,7-dimethoxy-2-methylindane

: 1417537-03-1
chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: (IPr)NiCl₂PPh₃ / tetrahydrofuran / 0.52 h / 20 °C / Reflux

1.2: Reflux

2.1: n-butyllithium / tetrahydrofuran; toluene; hexane / 16 h / -20 - 60 °C

With n-butyllithium; (IPr)NiCl₂PPh₃; In tetrahydrofuran; hexane; toluene;

Reference yield:

: 22385-77-9
1-bromo-3,5-di-tert-butylbenzene

: 1417537-03-1
chloro [4-(3,5-di-tert-butylphenyl)-7-methoxy-2-methyl-1H-inden-1-yl]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; tetrahydrofuran; toluene

2: tetrahydrofuran; toluene

With hydrogenchloride; In tetrahydrofuran; water; toluene;