(1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid

Base Information

• Chemical Name: (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid
• CAS No.: 1067652-72-5
• Molecular Formula: C₁₈H₂₆N₂O₅S
• Molecular Weight: 382.481

Synonyms:(1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid

Chemical Property of (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid

Chemical Property:

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Technology Process of (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid

There total 1 articles about (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1R,2R,4S)-2-[(S)-1-(4-chloro-phenyl)-ethylcarbamoyl]-4-(methanesulfonyl-methyl-amino)-cyclopentanecarboxylic acid methyl ester (1067652-29-2) → (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid (1067652-72-5)

Guidance literature:

(1R,2R,4S)-2-[(S)-1-(4-chloro-phenyl)-ethylcarbamoyl]-4-(methanesulfonyl-methyl-amino)-cyclopentanecarboxylic acid methyl ester; With methanol; lithium hydroxide; water;

With acetic acid; In ethyl acetate; toluene;

Reference yield:

(1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-2-[(S)-1-p-tolyl-ethylcarbamoyl]-cyclopentanecarboxylic acid (1067652-72-5) + (2R,4S,5S)-5-amino-6-(3,5-difluoro-phenoxy)-4-hydroxy-2-methoxy-hexanoic acid ((S)-1-benzylcarbamoyl-2-methyl-propyl)-amide (1067652-47-4) → (1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-cyclopentane-1,2-dicarboxylic acid 1-{[(1S,2S,4R)-4-((S)-1-benzylcarbamoyl-2-methyl-propylcarbamoyl)-1-(3,5-difluoro-phenoxymethyl)-2-hydroxy-4-methoxy-butyl]-amide} 2-[((S)-1-p-tolyl-ethyl)-amide] (1067651-51-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; for 4h;

upstream raw materials:

(1R,2R,4S)-2-[(S)-1-(4-chloro-phenyl)-ethylcarbamoyl]-4-(methanesulfonyl-methyl-amino)-cyclopentanecarboxylic acid methyl ester

Downstream raw materials:

(1R,2R,4S)-4-(methanesulfonyl-methyl-amino)-cyclopentane-1,2-dicarboxylic acid 1-{[(1S,2S,4R)-4-((S)-1-benzylcarbamoyl-2-methyl-propylcarbamoyl)-1-(3,5-difluoro-phenoxymethyl)-2-hydroxy-4-methoxy-butyl]-amide} 2-[((S)-1-p-tolyl-ethyl)-amide]

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