1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine

Base Information

• Chemical Name: 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine
• CAS No.: 89073-52-9
• Molecular Formula: C₂₀H₂₆N₆O₄S
• Molecular Weight: 446.53

Synonyms:1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine

Chemical Property of 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine

Chemical Property:

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Technology Process of 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine

There total 6 articles about 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-piperazine (109-01-3) + 4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)benzenesulfonic acid (89073-47-2) → 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine (89073-52-9)

Guidance literature:

With thionyl chloride; In water; N,N-dimethyl-formamide;

Reference yield:

5,6-diamino-1,3-diethyluracil (52998-22-8) → 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine (89073-52-9)

Guidance literature:

Multi-step reaction with 4 steps

1: ethyl <3-(dimethylamino)propyl>carbodiimide (EDAC) / H₂O

2: 30percent aq. KOH / 0.17 h / Heating

3: SOCl₂ / dimethylformamide / 0 - 20 °C

4: dimethylformamide / Ambient temperature

With potassium hydroxide; thionyl chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; N,N-dimethyl-formamide;

DOI:10.1021/jm00146a016

Reference yield:

4-sulphobenzoic acid (636-78-2,97993-77-6) → 1-[[4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)phenyl]sulfonyl]-4-methylpiperazine (89073-52-9)

Guidance literature:

Multi-step reaction with 4 steps

1: ethyl <3-(dimethylamino)propyl>carbodiimide (EDAC) / H₂O

2: 30percent aq. KOH / 0.17 h / Heating

3: SOCl₂ / dimethylformamide / 0 - 20 °C

4: dimethylformamide / Ambient temperature

With potassium hydroxide; thionyl chloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In water; N,N-dimethyl-formamide;

DOI:10.1021/jm00146a016

upstream raw materials:

1-methyl-piperazine

5,6-diamino-1,3-diethyluracil

4-sulphobenzoic acid

4-(1,3-diethyl-2,3,6,7-tetrahydro-2,6-dioxo-1H-purin-8-yl)benzenesulfonic acid

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