1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

Base Information

Chemical Name:1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide
CAS No.:1179329-57-7
Molecular Formula:C₂₈H₂₃F₄N₅O₆S
Molecular Weight:633.58
Hs Code.:

1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

Synonyms:1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

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Chemical Property of 1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

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Technology Process of 1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

There total 3 articles about 1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1006899-55-3
4-[3-(2-amino-4-fluorobenzyl)-4,4-dimethyl-2,5-dioxoimidazolidin-1-yl]-2-trifluoromethylbenzonitrile

: 400900-01-8
methyl 4-chlorosulfonylaminobenzoate

: 1179329-57-7
1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1179329-57-7
1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; chlorosulfonic acid / dichloromethane / 0 - 20 °C

2: phosphorus pentachloride / dichloromethane / 4 h / 20 °C

3: triethylamine / dichloromethane / 12 h / 20 °C

With chlorosulfonic acid; phosphorus pentachloride; triethylamine; In dichloromethane;

Reference yield:

: 611396-51-1
methyl 4-sulfoaminobenzoate sodium salt

: 1179329-57-7
1-{2-[3-(4-cyano-3-trifluoromethylphenyl)-5,5-dimethyl-2,4-dioxo-imidazolidin-1-ylmethyl]-5-fluorophenyl}-3-(4-methoxycarbonyl-phenyl)sulfamide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentachloride / dichloromethane / 4 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 20 °C

With phosphorus pentachloride; triethylamine; In dichloromethane;