1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene

Base Information

• Chemical Name: 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene
• CAS No.: 213135-26-3
• Molecular Formula: C₂₅H₂₈O₂S₃
• Molecular Weight: 456.694
• Mol file: 213135-26-3.mol

Synonyms:1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene

Chemical Property of 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene

There total 5 articles about 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-Bromo-3,5-bis-(4-isopropoxy-phenylsulfanyl)-benzene + sodium thiomethoxide (5188-07-8) → 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene (213135-26-3)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 4h;

DOI:10.1016/S0040-4039(98)01327-6

Reference yield: 40.0%

4-isopropyloxythiophenol (702-12-5) + (3,5-dibromophenyl)(methyl)sulfane (141938-37-6) → 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene (213135-26-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 150 ℃; for 3h;

DOI:10.1016/S0040-4039(98)01327-6

Reference yield:

4-isopropyloxythiophenol (702-12-5) → 1,3-Bis-(4-isopropoxy-phenylsulfanyl)-5-methylsulfanyl-benzene (213135-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NaH / dimethylformamide / 22 h / 100 °C

2: 90 percent / dimethylformamide / 4 h / 80 °C

With sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(98)01327-6

upstream raw materials:

4-isopropyloxythiophenol

(3,5-dibromophenyl)(methyl)sulfane

sodium thiomethoxide

3,5-difluorobromobenzene