1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

Base Information

Chemical Name:1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne
CAS No.:78131-62-1
Molecular Formula:C₂₄H₁₅ClFNO₃
Molecular Weight:419.839
Hs Code.:

Synonyms:1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

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Chemical Property of 1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

Chemical Property:

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Technology Process of 1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

There total 1 articles about 1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78131-62-1
1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

Guidance literature:

Reference yield:

: 78131-62-1
1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

: 83948-86-1
4-<4-chloro-2-<(2-fluorophenyl)hydroxymethyl>phenyl>-5-(N-phthalimidimethyl)-2H-1,2,3-triazole

Guidance literature:: With sodium azide; acetic acid; In dimethyl sulfoxide; at 90 ℃; for 96h;
DOI:10.1021/jm00357a011

Reference yield:

: 78131-62-1
1-{4-chloro-2-[(2-fluorophenyl)hydroxymethyl]phenyl}-3-phthalimidopropyne

: 78131-53-0
8-Chloro-6-(2-fluorophenyl)-2H,4H-[1,2,3]triazolo[4,5-d][2]benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.3 g / sodium azide, acetic acid / dimethylsulfoxide / 96 h / 90 °C

2: 60 percent / Jones reagent / acetone / 1 h / Ambient temperature

3: 88 percent / 40 percent aq. methylamine / ethanol / 12 h / Ambient temperature

With sodium azide; jones reagent; acetic acid; methylamine; In ethanol; dimethyl sulfoxide; acetone;
DOI:10.1021/jm00357a011