2-(phenylsulfonyl)-3-methoxy-1-propene

Base Information

Chemical Name:2-(phenylsulfonyl)-3-methoxy-1-propene
CAS No.:84363-84-8
Molecular Formula:C₁₀H₁₂O₃S
Molecular Weight:212.269
Hs Code.:

Synonyms:2-(phenylsulfonyl)-3-methoxy-1-propene

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Chemical Property of 2-(phenylsulfonyl)-3-methoxy-1-propene

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Technology Process of 2-(phenylsulfonyl)-3-methoxy-1-propene

There total 5 articles about 2-(phenylsulfonyl)-3-methoxy-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 84391-08-2
(2-Benzenesulfonyl-2-chloro-3-methoxy-propyl)-trimethyl-silane

: 84363-84-8
2-(phenylsulfonyl)-3-methoxy-1-propene

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 0.166667h;
DOI:10.1016/S0040-4039(00)87640-6

Reference yield:

: 73476-18-3
1-benzenesulfonyl-2-trimethylsilylethane

: 84363-84-8
2-(phenylsulfonyl)-3-methoxy-1-propene

Guidance literature:: Multi-step reaction with 5 steps

1: n-butyllithium / hexane; diethyl ether / -70 °C

2: 97 percent / CrO₃, H₂SO₄ / acetone / 1 h / 0 - 5 °C

3: 99 percent / KOH, NaOCl / dioxane / 2.5 h

4: n-butyllithium, HMPA / diethyl ether; hexane

5: 97 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h

With chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hydroxide; sodium hypochlorite; n-butyllithium; sulfuric acid; tetrabutyl ammonium fluoride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; acetone;
DOI:10.1016/S0040-4039(00)87640-6

Reference yield:

: 84363-74-6
1-(phenylsulfonyl)-1-chloro-2-(trimethylsilyl)ethane

: 84363-84-8
2-(phenylsulfonyl)-3-methoxy-1-propene

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium, HMPA / diethyl ether; hexane

2: 97 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.17 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/S0040-4039(00)87640-6