4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

Base Information

Chemical Name:4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine
CAS No.:157871-26-6
Molecular Formula:C₂₀H₁₇ClN₄O₄
Molecular Weight:412.832
Hs Code.:

Synonyms:4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

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Chemical Property of 4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

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Technology Process of 4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

There total 1 articles about 4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4316-93-2
4,6-dichloro-5-nitropyrimidine

: 112698-36-9
2-<(4-methoxybenzyl)amino>-1-phenylethanone

: 157871-26-6
4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

Guidance literature:: In chloroform; at 0 - 5 ℃; for 1h;
DOI:10.1248/cpb.43.408

Reference yield:

: 157871-26-6
4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

: 5-(N-hydroxyformamido)-4-<(4-methoxybenzyl)amino>-6-methylthiopyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) thiourea, 2.) aq. NH₃, 3.) aq. NaOH

2: 52 percent / 1 N aq. NaOH / methanol / 1 h / Ambient temperature

3: 16percent methanolic NH₃ / 4 h / 24 °C

With ammonium hydroxide; sodium hydroxide; ammonia; thiourea; In methanol;

Reference yield:

: 157871-26-6
4-chloro-6-<(4-methoxybenzyl)(2-oxo-2-phenylethyl)amino>-5-nitropyrimidine

: 8-amino-9-(4-methoxybenzyl)-6-methylthiopurine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) thiourea, 2.) aq. NH₃, 3.) aq. NaOH

2: 52 percent / 1 N aq. NaOH / methanol / 1 h / Ambient temperature

3: 18 percent / NH₃ / ethanol / 6 h / 110 °C

With ammonium hydroxide; sodium hydroxide; ammonia; thiourea; In methanol; ethanol;