(E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

Base Information

Chemical Name:(E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate
CAS No.:1422251-65-7
Molecular Formula:C₂₇H₃₄O₄
Molecular Weight:422.565
Hs Code.:

Synonyms:(E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

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Chemical Property of (E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

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Technology Process of (E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

There total 1 articles about (E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1416859-40-9
methyl 2-hydroxy-4-methoxy-6-(2-phenethyl)benzoate

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 1422251-65-7
(E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

: C₂₇H₃₄O₄

Guidance literature:: methyl 2-hydroxy-4-methoxy-6-(2-phenethyl)benzoate; With potassium hydride; In toluene; at 20 - 70 ℃; for 0.666667h; Schlenk technique; Inert atmosphere;

1-chloro-3,7-dimethylocta-2,6-diene; In toluene; at 80 ℃; for 2h; Molecular sieve; Schlenk technique; Inert atmosphere;
DOI:10.1021/jm3013272

Reference yield: 70.0%

: 1422251-65-7
(E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate

: (E)-3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-(2-phenethyl)benzoic acid

Guidance literature:: (E)-methyl 3-(3,7-dimethylocta-2,6-dien-1-yl)-2-hydroxy-4-methoxy-6-phenethylbenzoate; With potassium hydroxide; In methanol; water; at 78 ℃; for 7h;

With hydrogenchloride; In water; pH=3;
DOI:10.1021/jm3013272