N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

Base Information

Chemical Name:N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine
CAS No.:1358762-06-7
Molecular Formula:C₂₂H₂₂N₂S
Molecular Weight:346.496
Hs Code.:

Synonyms:N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

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Chemical Property of N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

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Technology Process of N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

There total 4 articles about N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 104-95-0
(4-bromophenyl)thioanisole

: 1278587-72-6
potassium 2-{[4-(dimethylamino)phenyl]imino}-2-phenylacetate

: 1358762-06-7
N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; magnesium triflate; copper(I) bromide; In 1-methyl-pyrrolidin-2-one; at 130 ℃; for 16h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.201101103

Reference yield:

: 99-98-9
4-amino-N,N-dimethylaniline

: 1358762-06-7
N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 16 h / 25 °C / Inert atmosphere

2: potassium tert-butylate / diethyl ether / 1 h / 25 °C / Inert atmosphere

3: 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; magnesium triflate; copper(I) bromide / 1-methyl-pyrrolidin-2-one / 16 h / 130 °C / Inert atmosphere; Molecular sieve

With 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; potassium tert-butylate; magnesium triflate; copper(I) bromide; In 1-methyl-pyrrolidin-2-one; methanol; diethyl ether;
DOI:10.1002/ejoc.201101103

Reference yield:

: 611-73-4
Benzoylformic acid

: 1358762-06-7
N,N-dimethyl-N'-[(4-methylsulfanylphenyl)(phenyl)methylene]-p-phenylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 16 h / 25 °C / Inert atmosphere

2: potassium tert-butylate / diethyl ether / 1 h / 25 °C / Inert atmosphere

3: 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; magnesium triflate; copper(I) bromide / 1-methyl-pyrrolidin-2-one / 16 h / 130 °C / Inert atmosphere; Molecular sieve

With 1,1'-bis-(diphenylphosphino)ferrocene; 1,10-Phenanthroline; palladium(II) hexafluoroacetylacetonate; potassium tert-butylate; magnesium triflate; copper(I) bromide; In 1-methyl-pyrrolidin-2-one; methanol; diethyl ether;
DOI:10.1002/ejoc.201101103