(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

Base Information

Chemical Name:(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl
CAS No.:863651-22-3
Molecular Formula:C₃₀H₃₀O₅
Molecular Weight:470.565
Hs Code.:

Synonyms:(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

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Chemical Property of (2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

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Technology Process of (2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

There total 2 articles about (2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 110-00-9
furan

: 52522-49-3
2,3,5-tri-O-benzyl-1-(4-nitrobenzoyloxy)-D-arabinofuranose

: 863651-22-3
(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

: (2S,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

Guidance literature:: With tin(IV) chloride; In dichloromethane; for 4h;
DOI:10.1021/jo0504159

Reference yield:

: 110-00-9
furan

: 863651-21-2
C₃₃H₃₃NO₇

: 863651-22-3
(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

: (2S,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 0 - 20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.10.041

Reference yield:

: 863651-22-3
(2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl

: (Z)-4-((2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yl)-4-oxo-but-2-enal

Guidance literature:: (2R,3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-2,3,4,5-tetrahydro-[2,2']bifuranyl; With oxygen; methylene blue; In methanol; at -20 ℃; UV-irradiation;

With diethyl sulphide; In methanol; at -20 ℃;
DOI:10.1021/jo0504159