C₅₁H₅₉N₉O₉

Base Information

Chemical Name:C₅₁H₅₉N₉O₉
CAS No.:1392101-95-9
Molecular Formula:C₅₁H₅₉N₉O₉
Molecular Weight:942.084
Hs Code.:

C<sub>51</sub>H<sub>59</sub>N<sub>9</sub>O<sub>9</sub>

Synonyms:C₅₁H₅₉N₉O₉

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Chemical Property of C₅₁H₅₉N₉O₉

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Technology Process of C₅₁H₅₉N₉O₉

There total 15 articles about C₅₁H₅₉N₉O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: C₃₇H₃₇N₇O₃*4ClH

: 111398-44-8,74761-42-5
N-methoxycarbonyl-L-valine

: 1392101-95-9
C₅₁H₅₉N₉O₉

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 3h;

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1392101-95-9
C₅₁H₅₉N₉O₉

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / ethanol / 6 h / Reflux

2: polyphosphoric acid / 2 h / 80 °C

3: caesium carbonate / dimethyl sulfoxide / 18 h / 90 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.75 h / 90 °C / Inert atmosphere; Microwave irradiation

5: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 17 h / 90 °C

6: hydrogenchloride / 1,4-dioxane; methanol / 23 h / 20 °C

7: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 3 h / 0 °C

With hydrogenchloride; potassium acetate; potassium carbonate; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; HATU; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 69610-41-9,117625-90-8
Boc-L-Pro-H

: 1392101-95-9
C₅₁H₅₉N₉O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonia / methanol / 0.5 h / 20 - 30 °C

1.2: 16 h / 20 - 60 °C

2.1: N-Bromosuccinimide / dichloromethane / 1.25 h / Cooling with ice

3.1: potassium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane; water / 17 h / 90 °C

4.1: hydrogenchloride / 1,4-dioxane; methanol / 23 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 3 h / 0 °C

With hydrogenchloride; N-Bromosuccinimide; ammonia; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;