(E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester

Base Information

• Chemical Name: (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester
• CAS No.: 1185745-14-5
• Molecular Formula: C₃₉H₅₆O₁₂Si₂
• Molecular Weight: 773.037

Synonyms:(E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester

Chemical Property of (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester

There total 1 articles about (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(E)-1-{[3-tert-butyl(dimethyl)silyl]oxy}-5-hydroxyphenyl-2-({[4-tert-butyl(dimethyl)silyl]oxy}-phenyl)ethene (827348-01-6) + methyl 2,3,4-tri-O-acetyl-α,β-D-glucopyranosyluronate trichloroacetimidate → (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester (1185745-14-5)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at -10 ℃; for 1.5h;

DOI:10.1016/j.carres.2009.05.016

Reference yield: 80.0%

(E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester (1185745-14-5) → C27H28O12 (827026-54-0)

Guidance literature:

With pyridine; hydrogen fluoride; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1016/j.carres.2009.05.016

upstream raw materials:

(E)-1-{[3-tert-butyl(dimethyl)silyl]oxy}-5-hydroxyphenyl-2-({[4-tert-butyl(dimethyl)silyl]oxy}-phenyl)ethene

Downstream raw materials:

C₂₇H₂₈O₁₂

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1185745-14-5 (E)-1-[3-tert-butyldimethylsilyloxy-5-O-(2,3,4-tri-O-acetyl-β-D-glucopyranoside)phenyl]-2-(4'-tert-butyldimethylsilyloxyphenyl)ethene methyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send