C₁₄H₉ClN₆O₃

Base Information

Chemical Name:C₁₄H₉ClN₆O₃
CAS No.:1374779-66-4
Molecular Formula:C₁₄H₉ClN₆O₃
Molecular Weight:344.717
Hs Code.:

C<sub>14</sub>H<sub>9</sub>ClN<sub>6</sub>O<sub>3</sub>

Synonyms:C₁₄H₉ClN₆O₃

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Chemical Property of C₁₄H₉ClN₆O₃

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Technology Process of C₁₄H₉ClN₆O₃

There total 3 articles about C₁₄H₉ClN₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374779-65-3
C₁₄H₈ClN₃O₃

: 1374779-66-4
C₁₄H₉ClN₆O₃

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 100 ℃; for 24h;

Reference yield:

: 939-79-7
4-cyano-2-nitrotoluene

: 1374779-66-4
C₁₄H₉ClN₆O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium dichromate; sulfuric acid / 5 h / 0 - 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

2.2: 12 h / 20 °C

3.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 100 °C

With sodium azide; sodium dichromate; oxalyl dichloride; sulfuric acid; ammonium chloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 64629-99-8
4-cyano-2-nitrobenzoic acid

: 1374779-66-4
C₁₄H₉ClN₆O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 4 h / 20 °C

1.2: 12 h / 20 °C

2.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 100 °C

With sodium azide; oxalyl dichloride; ammonium chloride; N,N-dimethyl-formamide; In dichloromethane; N,N-dimethyl-formamide;