Technology Process of C28H32N2O12S
There total 7 articles about C28H32N2O12S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C28H30N2O14S;
With
hydrogenchloride; tin(ll) chloride;
In
methanol; water;
at 20 ℃;
for 12h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
pH=8 - 9;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: silver(l) oxide / acetonitrile / 12 h / 20 °C / Darkness; Inert atmosphere
2.1: sodium tetrahydroborate / isopropyl alcohol; chloroform / 12 h / 0 - 20 °C / Inert atmosphere
3.1: dmap / dichloromethane / 12 h / 20 °C
4.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere
5.1: dichloromethane / 2 h / 20 °C / Inert atmosphere
6.1: hydrogenchloride; tin(ll) chloride / water; methanol / 12 h / 20 °C
6.2: pH 8 - 9
With
hydrogenchloride; dmap; sodium tetrahydroborate; tin(ll) chloride; silver(l) oxide;
In
methanol; dichloromethane; chloroform; water; isopropyl alcohol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloromethane / 0.17 h / 20 °C / Inert atmosphere
2.1: dichloromethane / 2 h / 20 °C / Inert atmosphere
3.1: hydrogenchloride; tin(ll) chloride / water; methanol / 12 h / 20 °C
3.2: pH 8 - 9
With
hydrogenchloride; tin(ll) chloride;
In
methanol; dichloromethane; water;