N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

Base Information

Chemical Name:N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane
CAS No.:129839-57-2
Molecular Formula:C₅₄H₇₀N₂O₁₂
Molecular Weight:939.156
Hs Code.:

Synonyms:N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

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Chemical Property of N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

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Technology Process of N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

There total 7 articles about N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 82052-55-9
4-(4-Heptyloxy-benzoyloxy)-benzoyl-chlorid

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 129839-57-2
N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

Guidance literature:: With triethylamine; In benzene; for 16h; Heating;
DOI:10.1021/jp990787j

Reference yield:

: 25804-49-3
tert-butyl 4-hydroxybenzoate

: 129839-57-2
N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Et₃N / benzene / 12 h / 20 °C

2: 74 percent / TFA; anisole / CH₂Cl₂ / 3 h / 0 °C

3: SOCl₂ / 16 h / Heating

4: 88 percent / Et₃N / benzene / 16 h / Heating

With thionyl chloride; methoxybenzene; triethylamine; trifluoroacetic acid; In dichloromethane; benzene; 1: Acylation / 2: Hydrolysis / 3: Substitution / 4: Acylation;
DOI:10.1021/jp990787j

Reference yield:

: 40782-54-5
4-heptyloxybenzoyl chloride

: 129839-57-2
N,N-bis<4-(4-heptoxybenzoyloxy)benzoyl>-1,10-diaza-4,7,13,16-tetracyclooxaotadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Et₃N / benzene / 12 h / 20 °C

2: 74 percent / TFA; anisole / CH₂Cl₂ / 3 h / 0 °C

3: SOCl₂ / 16 h / Heating

4: 88 percent / Et₃N / benzene / 16 h / Heating

With thionyl chloride; methoxybenzene; triethylamine; trifluoroacetic acid; In dichloromethane; benzene; 1: Acylation / 2: Hydrolysis / 3: Substitution / 4: Acylation;
DOI:10.1021/jp990787j