N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

Base Information

Chemical Name:N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt
CAS No.:131235-53-5
Molecular Formula:C₁₂H₁₁F₃NO₆S*K
Molecular Weight:393.382
Hs Code.:

Synonyms:N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

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Chemical Property of N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

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Technology Process of N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

There total 5 articles about N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 102422-54-8
m-(trifluoromethyl)phenylalanine methyl ester isocyanate

: 131235-53-5
N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

Guidance literature:: With potassium disulphite; In 1,4-dioxane; water; Ambient temperature;
DOI:10.1021/jm00157a034

Reference yield:

: 102422-51-5
diethyl (m-(trifluoromethyl)benzyl)formamidomalonate

: 131235-53-5
N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / 10percent HCl / 4 h / Heating

2: 82 percent / thionyl chloride / 2 h

3: 84 percent / dioxane / Heating

4: 92 percent / potassium metabisulfite / dioxane; H₂O / Ambient temperature

With hydrogenchloride; potassium disulphite; thionyl chloride; In 1,4-dioxane; water;
DOI:10.1021/jm00157a034

Reference yield:

: 3832-76-6
m-(trifluoromethyl)phenylalanine hydrochloride

: 131235-53-5
N-(sulfocarbonyl)-DL-m-(trifluoromethyl)phenylalanine methyl ester, monopotassium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / thionyl chloride / 2 h

2: 84 percent / dioxane / Heating

3: 92 percent / potassium metabisulfite / dioxane; H₂O / Ambient temperature

With potassium disulphite; thionyl chloride; In 1,4-dioxane; water;
DOI:10.1021/jm00157a034