C₉H₁₂N₂O₄

Base Information

• Chemical Name: C₉H₁₂N₂O₄
• CAS No.: 1187660-27-0
• Molecular Formula: C₉H₁₂N₂O₄
• Molecular Weight: 212.205
• Mol file: 1187660-27-0.mol

Synonyms:C₉H₁₂N₂O₄

Chemical Property of C₉H₁₂N₂O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₉H₁₂N₂O₄

There total 1 articles about C₉H₁₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.8%

C17H14N2O6 (1187660-26-9) → C9H12N2O4 (1187660-27-0)

Guidance literature:

With hydrazine hydrate; In ethanol; at 50 ℃; for 1h;

Reference yield: 66.6%

di-tert-butyl dicarbonate (24424-99-5) + C9H12N2O4 (1187660-27-0) → C14H20N2O6 (1187660-28-1)

Guidance literature:

With triethylamine; In 1,4-dioxane; at 20 ℃;

Reference yield:

C9H12N2O4 (1187660-27-0) → C26H32N4O7S (1187660-73-6)

Guidance literature:

Multi-step reaction with 4 steps

1: triethylamine / 1,4-dioxane / 20 °C

2: hydrogen / palladium on activated charcoal / tetrahydrofuran; thiophene; di-isopropyl ether / 20 h / 20 °C

3: toluene-4-sulfonic acid / 1,4-dioxane / 20 h / 100 °C

4: N-ethyl-N,N-diisopropylamine / acetonitrile / 20 °C

With hydrogen; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; thiophene; di-isopropyl ether; acetonitrile;

upstream raw materials:

C₁₇H₁₄N₂O₆

Downstream raw materials:

C₁₄H₂₀N₂O₆

C₁₄H₂₂N₂O₄

C₂₅H₃₀N₄O₅

C₂₃H₂₇N₅O₅