C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

Base Information

Chemical Name:C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)
CAS No.:1425265-69-5
Molecular Formula:C₁₃H₂NO₂S₆*C₂₄H₂₀B
Molecular Weight:715.794
Hs Code.:

C<sub>13</sub>H<sub>2</sub>NO<sub>2</sub>S<sub>6</sub><sup>(1+)</sup>*C<sub>24</sub>H<sub>20</sub>B<sup>(1-)</sup>

Synonyms:C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

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Chemical Property of C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

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Technology Process of C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

There total 6 articles about C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 3.0%

: 1425265-61-7
3,4,6,7-tetrathio-9-hydroxyphenalen-1-one

: 143-66-8
sodium tetraphenyl borate

: 1425265-69-5
C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

Guidance literature:: 3,4,6,7-tetrathio-9-hydroxyphenalen-1-one; With Lawessons reagent; In chlorobenzene; at 135 ℃; for 36h; Inert atmosphere; Schlenk technique;

sodium tetraphenyl borate; In methanol; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol400452f

Reference yield:

: 1425265-59-3
3,4,6,7-tetrakis(methanesulfonyloxy)-9-hydroxyphenalen-1-one

: 1425265-69-5
C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium thioacetate / N,N-dimethyl-formamide / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2.1: Lawessons reagent / chlorobenzene / 36 h / 135 °C / Inert atmosphere; Schlenk technique

2.2: 20 °C / Inert atmosphere; Schlenk technique

With Lawessons reagent; potassium thioacetate; In N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/ol400452f

Reference yield:

: 17276-03-8
1,3,6,8-tetramethoxynaphthalene

: 1425265-69-5
C₁₃H₂NO₂S₆⁽¹⁺⁾*C₂₄H₂₀B^(1-)

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique

1.2: 18 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: hydrogenchloride; water / 20 - 85 °C / Inert atmosphere; Schlenk technique

3.1: pyridine hydrochloride / 4 h / 180 °C / Inert atmosphere; Schlenk technique

4.1: triethylamine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Schlenk technique

4.2: 20 °C / Inert atmosphere

5.1: potassium thioacetate / N,N-dimethyl-formamide / 72 h / 20 °C / Inert atmosphere; Schlenk technique

6.1: Lawessons reagent / chlorobenzene / 36 h / 135 °C / Inert atmosphere; Schlenk technique

6.2: 20 °C / Inert atmosphere; Schlenk technique

With Lawessons reagent; hydrogenchloride; water; pyridine hydrochloride; triethylamine; potassium thioacetate; In dichloromethane; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/ol400452f