C₆₃H₆₇⁽²⁾HO₁₀

Base Information

Chemical Name:C₆₃H₆₇⁽²⁾HO₁₀
CAS No.:139195-47-4
Molecular Formula:C₆₃H₆₈O₁₀
Molecular Weight:986.219
Hs Code.:

C<sub>63</sub>H<sub>67</sub><sup>(2)</sup>HO<sub>10</sub>

Synonyms:C₆₃H₆₇⁽²⁾HO₁₀

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₆₇⁽²⁾HO₁₀

Chemical Property:

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Technology Process of C₆₃H₆₇⁽²⁾HO₁₀

There total 4 articles about C₆₃H₆₇⁽²⁾HO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: C₆₅H₆₉⁽²⁾HO₁₁S₂

: 139195-47-4
C₆₃H₆₇⁽²⁾HO₁₀

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 120 ℃; for 0.166667h;
DOI:10.1021/jo00022a039

Reference yield:

: 89160-12-3
C₆₃H₆₄O₁₀

: 139195-47-4
C₆₃H₆₇⁽²⁾HO₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂, quinoline / Lindlar catalyst / ethyl acetate / 0.33 h / Ambient temperature

2: 1.) BD₃*THF, 2.) 10percent aq. NaOH, 30percent H₂O₂ / 1.) THF, room temperature, overnight, 2.) THF, room temperature, 2 h

4: 89 percent / tributyltin hydride, AIBN / toluene / 0.17 h / 120 °C

With quinoline; sodium hydroxide; 2,2'-azobis(isobutyronitrile); borane-d3-tetrahydrofuran; hydrogen; dihydrogen peroxide; tri-n-butyl-tin hydride; Lindlar's catalyst; In ethyl acetate; toluene;
DOI:10.1021/jo00022a039

Reference yield:

: 139195-45-2
(Z)-methyl 8,12-anhydro-2,3,4,9,10,11,13-hepta-O-benzyl-6,7-dideoxy-α-D-glycero-D-gulo-tridec-6-enopyranoside

: 139195-47-4
C₆₃H₆₇⁽²⁾HO₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BD₃*THF, 2.) 10percent aq. NaOH, 30percent H₂O₂ / 1.) THF, room temperature, overnight, 2.) THF, room temperature, 2 h

3: 89 percent / tributyltin hydride, AIBN / toluene / 0.17 h / 120 °C

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); borane-d3-tetrahydrofuran; dihydrogen peroxide; tri-n-butyl-tin hydride; In toluene;
DOI:10.1021/jo00022a039