Technology Process of C20H19NO2
There total 6 articles about C20H19NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
C11H15N3Ru(2+)*2F6Sb(1-); oxygen; copper(II) acetate monohydrate;
at 60 ℃;
for 15h;
DOI:10.1021/ol501599j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / toluene / 2 h / 20 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
3: zinc; acetic acid / dichloromethane / 0 °C
4: triethylamine / tetrahydrofuran / 0 °C
5: C11H15N3Ru(2+)*2F6Sb(1-); copper(II) acetate monohydrate; oxygen / 15 h / 60 °C
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; di-isopropyl azodicarboxylate; C11H15N3Ru(2+)*2F6Sb(1-); oxygen; copper(II) acetate monohydrate; acetic acid; triethylamine; triphenylphosphine; zinc;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol501599j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / toluene / 2 h / 20 °C
2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C
3: zinc; acetic acid / dichloromethane / 0 °C
4: triethylamine / tetrahydrofuran / 0 °C
5: C11H15N3Ru(2+)*2F6Sb(1-); copper(II) acetate monohydrate; oxygen / 15 h / 60 °C
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; di-isopropyl azodicarboxylate; C11H15N3Ru(2+)*2F6Sb(1-); oxygen; copper(II) acetate monohydrate; acetic acid; triethylamine; triphenylphosphine; zinc;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ol501599j