tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

Base Information

Chemical Name:tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate
CAS No.:1082953-59-0
Molecular Formula:C₂₉H₃₇N₃O₆S
Molecular Weight:555.695
Hs Code.:

Synonyms:tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

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Chemical Property of tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

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Technology Process of tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

There total 4 articles about tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1082953-58-9
(Z)-tert-butyl 6-(4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

: 134-96-3
syringic aldehyde

: 1082953-59-0
tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

Guidance literature:: With piperidine; In ethanol; hexane; for 19h; Inert atmosphere; Reflux;
DOI:10.1021/jm8004515

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 1082953-59-0
tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 3 h / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

3: piperidine / ethanol / 19 h / Reflux; Inert atmosphere

With piperidine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;

Reference yield:

: 51857-17-1
tert-butyl N-(6-aminohexyl)carbamate

: 1082953-59-0
tert-butyl 6-((2Z,5Z)-6-(4-hydroxy-3,5-dimethoxybenzylidene)-4-oxo-2-(phenylimino)thiazolidin-3-yl)hexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 3 h / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

3: piperidine / ethanol / 19 h / Reflux; Inert atmosphere

With piperidine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;