tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

Base Information

Chemical Name:tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate
CAS No.:425686-78-8
Molecular Formula:C₁₉H₂₆F₃NO₃S
Molecular Weight:405.482
Hs Code.:

Synonyms:tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

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Technology Process of tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

There total 1 articles about tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75999-66-5
N-(4-methoxyphenyl)trifluoroacetimidoyl chloride

: 49827-07-8
tert-butyl α-tert-butylthioacetate

: 425686-78-8
tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 0 ℃;
DOI:10.1021/jo016108u

Reference yield: 72.0%

: 425686-78-8
tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

: tert-butyl 3-[N-(4-methoxyphenyl)amino]-2-tert-butylthio-4,4,4-trifluorobutanoate

: tert-butyl 3-[N-(4-methoxyphenyl)amino]-2-(tert-butylthio)-4,4,4-trifluorobutanoate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; diethylene glycol dimethyl ether; at 20 ℃; for 3h;
DOI:10.1021/jo016108u

Reference yield: 70.0%

: 425686-78-8
tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate

: tert-butyl 3-[N-(4-methoxyphenyl)amino]-2-tert-butylthio-4,4,4-trifluorobutanoate

Guidance literature:: tert-butyl 2-(tert-butylthio)-3-[N-(4-methoxyphenyl)imino]-4,4,4-trifluorobutanoate; With zinc dibromide; In dichloromethane; at 0 ℃; for 1h;

With sodium tetrahydroborate; In dichloromethane; at 20 ℃; for 1h; Further stages.;
DOI:10.1021/jo016108u