4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

Base Information

Chemical Name:4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine
CAS No.:130673-53-9
Molecular Formula:C₄₀H₆₂NO₂P
Molecular Weight:619.912
Hs Code.:

Synonyms:4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

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Chemical Property of 4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

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Technology Process of 4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

There total 5 articles about 4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₁H₃₀ClOP

: 130673-53-9
4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 4 h / 0 °C

2: 1) LDA / 1) THF, -78 deg C

3: (COCl)2

4: CH₂Cl₂ / 0 °C

With oxalyl dichloride; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1016/S0040-4039(00)97744-X

Reference yield:

: 130649-54-6
Methyl E,E-farnesylphenylphosphinate

: 130673-53-9
4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

Guidance literature:: Multi-step reaction with 5 steps

1: (COCl)2 / CH₂Cl₂ / 6 h / 0 °C

2: Et₃N / CH₂Cl₂ / 4 h / 0 °C

3: 1) LDA / 1) THF, -78 deg C

4: (COCl)2

5: CH₂Cl₂ / 0 °C

With oxalyl dichloride; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1016/S0040-4039(00)97744-X

Reference yield:

: Phenyl-((2E,6E)-3,7,11-trimethyl-dodeca-2,6,10-trienyl)-phosphinic acid (2E,6E)-3,6,11-trimethyl-dodeca-2,6,10-trienyl ester

: 130673-53-9
4-{Phenyl-[(3E,7E)-4,8,12-trimethyl-1-((1E,5E)-2,6,10-trimethyl-undeca-1,5,9-trienyl)-trideca-3,7,11-trienyl]-phosphinoyl}-morpholine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LDA / 1) THF, -78 deg C

2: (COCl)2

3: CH₂Cl₂ / 0 °C

With oxalyl dichloride; lithium diisopropyl amide; In dichloromethane;
DOI:10.1016/S0040-4039(00)97744-X